Document Type

Thesis

Date of Award

6-30-1959

Degree Name

Master of Science in Chemical Engineering - (M.S.)

Department

Chemical Engineering

First Advisor

Carl W. Carlson

Second Advisor

George C. Keeffe

Third Advisor

Saul I. Kreps

Abstract

This report is an investigation of the use of ion exchange resins to recover germanium from acid etch wastes encountered in transistor manufacture.

Most of the experiments were performed with acid etch waste of unknown germanium content. The object was to determine if the ion exchange technique were applicable, and to select the most practical operating procedure.

When a satisfactory procedure had been established, later experimental runs were made with an acid etch solution of known germanium concentration to determine the yields of recovered germanium.

Yields of 60 per cent to 75 per cent recovery of germanium from the etch waste were accomplished by eluting the germanium complex from a weakly base anion resin with a dilute ammonium hydroxide solution.

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