Document Type

Thesis

Date of Award

6-30-1959

Degree Name

Master of Science in Chemical Engineering - (M.S.)

Department

Chemical Engineering

First Advisor

Saul I. Kreps

Second Advisor

C. L. Mantell

Third Advisor

Joseph Joffe

Abstract

The factors governing the electrolytic reduction of ethyl para-nitrobenzoate have been investigated, and conditions established for the optimum yield of the end-product benzocaine. The formation of intermediate compounds was studied, and a mechanism for the reduction favoring the mono-molecular route has been suggested. The material costs of the electrolytic reduction have been shown to compare favorably with the material costs of a chemical reduction, such as the Bechamp process.

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