Document Type
Thesis
Date of Award
6-30-1957
Degree Name
Master of Science in Chemical Engineering - (M.S.)
Department
Chemical Engineering
First Advisor
C. L. Mantell
Second Advisor
Saul I. Kreps
Third Advisor
James A. Bradley
Abstract
This work presents data for the separation of materials involved in the chlorosulfonation of benzene using carbon tetrachloride as an inert extraction solvent. Equilibrium and tie line data for the liquid ternary systems; carbon tetrachloride chlorosulfonic acid - sulfuric acid; Benzenesulfonyl chloride - carbon tetrachloride - sulfuric acid; benzenesulfonyl chloride ehiorosulfonic acid - sulfuric acid and for the quaternary system benzenesulfonyl chloride - carbon tetrachloride chlorosulfonic acid - sulfuric acid have been determined. The tie line data has been correlated by the method of Othmer and Tobias.
Data for two chlorosulfonations made under differing conditions is also given.
Recommended Citation
Wiegleb, Ernest Eugene, "Continuous chlorosulfonation of benzene II phase relations" (1957). Theses. 2617.
https://digitalcommons.njit.edu/theses/2617
