Novel modifiers for layered double hydroxides and their effects on the properties of polylactic acid composites
Document Type
Article
Publication Date
2-1-2010
Abstract
Hydrophobic modification of a carbonated layered double hydroxide (LDH) and its calcined equivalent was conducted by direct ion exchange reactions with three ionic liquids having the same phosphonium-based cation, but different anions. Among the ionic liquids, successful anionic intercalation was only carried out when calcined LDH reacted with a phosphinate anion containing ionic liquid, in excess of the stoichiometric amount. Ionic liquids containing a linear decanoate anion or the least bulky PF6 anion promoted the formation of a surface coating rather than increase of the interlayer space as confirmed by X-ray Diffraction, Infrared Spectroscopy, and Thermogravimetric analysis. The intercalated LDH was found to minimize the plasticizing/degradative effect of the ionic liquid on a polylactic acid PLA matrix and could be used as reservoir for the controlled release of the phosphorous containing anions for antibacterial or similar applications. © 2009 Elsevier B.V. All rights reserved.
Identifier
75349107254 (Scopus)
Publication Title
Applied Clay Science
External Full Text Location
https://doi.org/10.1016/j.clay.2009.11.033
ISSN
01691317
First Page
303
Last Page
310
Issue
3-4
Volume
47
Recommended Citation
Ha, Jin Uk and Xanthos, Marino, "Novel modifiers for layered double hydroxides and their effects on the properties of polylactic acid composites" (2010). Faculty Publications. 6408.
https://digitalcommons.njit.edu/fac_pubs/6408
