Document Type

Thesis

Date of Award

9-30-1989

Degree Name

Master of Science in Chemical Engineering - (M.S.)

Department

Chemical Engineering, Chemistry and Environmental Science

First Advisor

Piero M. Armenante

Second Advisor

Henry Shaw

Third Advisor

Dana E. Knox

Abstract

The agitation requirements for complete drawdown of floating solids in mechanically agitated tank vessels has been studied both theoretically and experimentally.

A semi-theoretical equation has been derived on the basis of Kolmogoroff's theory of isotropic turbulence to determine the minimum impeller speed required for drawdown. The equation contains one adjustable parameter which has been found to be a function of the impeller type and position in the tank vessel.

The equation was tested using various vessels and impeller configurations. The solid phase consisted of high density polyethylene (density = 897kg/m3), low density polyethylene (density = 840kg/m3) and cork material (density = 510kg/m3) with particle sizes ranging from 300µm to 2200µm. The liquid phase consisted of water and aqueous solutions of zinc chloride in different concentrations so that the liquid density could be varied in the range 996kg/m3-1180kg/m3.

The effect of impeller position and pumping direction has been extensivelly examined, as well as the use of non-conventional baffling systems to facilitate the drawdown of floating particles into the liquid.

It was concluded that impeller clearance and pumping direction have a considerable influence over the minimum drawdown speed and its corresponding power consumption. A partial baffling system consisting of four half baffles has been found to have the lowest power requirements.

Noticeable similarities exist between settling solids suspensions and floating solids drawdown, particularly for floating particles which, at rest, are almost completely immersed in the liquid. For cases different from this, the suspension of floating solids becomes a three phase system with entrapped air playing a significant role in particle drawdown. The proposed model works well within the experimental range covered (i.e. small density difference ( < 340kg/m3) and medium particle size (300 - 2500µm)) and can be used to predict the performance of floating solid-liquid systems.

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